Related Products of 2687-12-9,Some common heterocyclic compound, 2687-12-9, name is Cinnamyl chloride, molecular formula is C9H9Cl, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
In the reaction (R10), the compound (A1-1) was reacted with triethyl phosphite to obtain a compound (B1-1). Specifically, 15.2 g (0.10 mol) of the compound (A1-1) and 25.0 g (0.15 mol) of triethyl phosphite were added to a flask having a capacity of 200 mL. The content of the flask was stirred at 180 C. for 8 hours and then cooled to room temperature. Subsequently, unreacted triethyl phosphite contained in the content of the flask was distilled off under reduced pressure. Thereby, a compound (B1-1) which is a white liquid was obtained. The yield of the compound (B1-1) was 22.9 g, and the yield of the compound (B1-1) from the compound (A1-1) was 90%.
These compound has a wide range of applications. It is believed that with the continuous development of the source of the synthetic route Cinnamyl chloride, its application will become more common.
Reference:
Patent; Kyocera Document Solutions Co., Ltd.; Okada, Hideki; (38 pag.)JP2018/95596; (2018); A;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics