Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 53531-69-4, name is (4-Bromophenyl)methanesulfonyl chloride, A new synthetic method of this compound is introduced below., Application In Synthesis of (4-Bromophenyl)methanesulfonyl chloride
General procedure: Two-step one-pot method: Add bromobenzyl mercaptan to acetonitrile, then add chlorinating reagent, monitor with spot plate, and transfer to ice water bath after reaction.Add 4 equivalents of an acid binding agent such as pyridine.After slowly adding 7-amino-N-propylquinolinone in acetonitrile,The plate is monitored for reaction, after the reaction, pickling, drying,Further, the abscisic acid receptor agonist can be obtained by column chromatography or recrystallization,
The synthetic route of 53531-69-4 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Shaoyang University; Huang Zhiyou; (7 pag.)CN109678797; (2019); A;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics