In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 6579-54-0, name is 2,6-Dichlorobenzenesulfonyl chloride belongs to chlorides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. category: chlorides-buliding-blocks
General procedure: To a solution of 1-(3-Amino-phenyl)-3-(4-hydroxy-3-methoxy-phenyl)-propenone (1) (0.1 g, 0.373 mmol) in 2.5 mL of dioxane/H2O (50:50) was added methanesulfonyl chloride (0.043 g, 0.372 mmol) over a 20 min period at 0 C followed by 5 h of vigorous stirring at room temperature. The solvent was removed in vacuo, and the resulting solid was purified by silica gel column chromatography (CHCl3/methanol = 95:5).
The synthetic route of 6579-54-0 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Park, Chong-Bin; Ahn, Chan Mug; Oh, Sangtae; Kwon, Daeho; Cho, Won-Chul; Shin, Woon-Seob; Cui, Yuan; Um, Ye Sol; Park, Byong-Gon; Lee, Seokjoon; Bioorganic and Medicinal Chemistry; vol. 23; 20; (2015); p. 6673 – 6682;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics