Recently I am researching about PRIMARY AMINES; INTERMOLECULAR HYDROAMINOALKYLATION; REDUCTIVE AMINATION; SELECTIVE SYNTHESIS; ONE-POT; EFFICIENT; NITRILES; ALKENES; N-(CYCLOHEXYLMETHYL)-N-ALKYLAMINES; TETRACARBONYLHYDRIDOFERRATE, Saw an article supported by the Natural Science Foundation of Jiangsu ProvinceNatural Science Foundation of Jiangsu Province [BK 20131346, BK 20140776]; National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21476116, 21402093]; Chinese Postdoctoral Science FoundationChina Postdoctoral Science Foundation [2015M571761, 2016T90465]. HPLC of Formula: C7H7Cl. Published in AMER CHEMICAL SOC in WASHINGTON ,Authors: Li, ZL; Sun, KK; Wu, PY; Cai, C. The CAS is 95-49-8. Through research, I have a further understanding and discovery of 1-Chloro-2-methylbenzene
The iron-catalyzed alpha-C-H alkylation of N-methylanilines without any directing group by cross-dehydrogenative coupling between unactivated C(sp(3))-H and C(sp(3))-H bonds has been established for the first time, which provides a good complement to C(sp(3))-H activation reactions and expands the field of Fe-catalyzed C-H functionalizations. Many different C(sp(3))-H bonds in cyclic alkanes, cyclic ethers, and toluene derivatives can be used as coupling partners. Mechanistic investigations including the radical reaction process, the main role of various reagents, and the kinetic isotope effect experiment were also described.
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Reference:
Patent; Nanjing Zhongteng Chemical Co., Ltd.; Zhong Hua; Lu Minshan; Chen Xiuzhen; Liu Qiaobao; Yin Hengbo; Wang Aili; (8 pag.)CN104876790; (2017); B;,
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