Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 2687-12-9, name is Cinnamyl chloride, A new synthetic method of this compound is introduced below., Safety of Cinnamyl chloride
To a solution of 2.94 g (0.02 mol) of isatin in 20 mL of DMF with stirring at 10C was slowly added 0.84 g (0.02 mol) of sodium hydride (60% suspension in mineral oil). After 30 min, 2.92 mL (0.02 mol) of cinnamyl chloride was added to the resulting purple solution followed by stirring at room temperature for 3 h. The reaction mixture was poured into 100 g of crushed ice. Next, the resulting precipitate was filtered off, washed with hexane, and dried in a vacuum(18 mmHg).
The synthetic route of 2687-12-9 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Bogdanov; Sadykov; Musin; Khamatgalimov; Krivolapov; Dobrynin; Mironov; Russian Journal of General Chemistry; vol. 85; 9; (2015); p. 2030 – 2036; Zh. Obshch. Khim.; vol. 85; 9; (2015); p. 1446 – 1452,7;,
Chloride – Wikipedia,
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