Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 626-43-7, name is 3,5-Dichloroaniline, This compound has unique chemical properties. The synthetic route is as follows., 626-43-7
Benzoyl acetone (0.165 g, 1.017 mmol) was dispersed over Montmorillonite K-10 catalyst (1.5 g) and a mixture of 3.5-dichloroaniline (0.552 g, 3.407 mmol) with 20 ml THF was added dropwise, while stirring. The reaction was stirred at room temperature for 48 h. The catalyst was removed by filtration and the solvent was removed on a rotary evaporator, yielding a dark red oil.Yield 93%. Colour: dark red. UV: lambdamax 359 nm, epsilonmax 29453 mol-1dm3cm-1 (CH3CN), 1H NMR (300 MHz, CDCl3, 25C):delta 7.91-7.89 ppm (d, aromatic, 2H); 7.54-7.44 ppm (m, aromatic,3H); 6.75-6.74 ppm (t, aromatic, 1H); 6.56 ppm (d, aromatic, 2H);6.20 ppm (s, CH, 1H); 2.22 ppm (s, CH3, 3H).
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Reference:
Article; Ngake, Tankiso Lawrence; Potgieter, Johannes Hermanus; Conradie, Jeanet; Electrochimica Acta; vol. 296; (2019); p. 1070 – 1082;,
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