Cragin, David W. published the artcileThe synthesis of 2-14C-N-nitrosothiazolidine, Computed Properties of 1002-41-1, the publication is Journal of Labelled Compounds and Radiopharmaceuticals (1989), 27(7), 777-81, database is CAplus.
Title compound I, labeled with 14C in the 2-position, was prepared in 30.7% yield by cyclocondensation of NH2CH2CH2SH with 14C-labeled CH2O in H2O at pH = 8, followed by nitrosylation of the thiazolidine with NaNO2 at pH = 4.5 adjusted with H2SO4. Adjustment of the pH in the latter step with HCl forms many disulfide byproducts.
Journal of Labelled Compounds and Radiopharmaceuticals published new progress about 1002-41-1. 1002-41-1 belongs to chlorides-buliding-blocks, auxiliary class Aliphatic Chain, name is 1,2-Bis(2-chloroethyl)disulfane, and the molecular formula is C4H8Cl2S2, Computed Properties of 1002-41-1.
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