Strzelczyk, Marek published the artcileSynthesis of 7-9-membered heterocyclic systems containing nitrogen and sulfur with expected pharmacological activity. I. Synthesis of perhydro-1,4,5-thiadiazocine, -1,4,6-thiadiazonine, and -1,2,5,7-dithiadiazonine derivatives, Name: 1,2-Bis(2-chloroethyl)disulfane, the publication is Acta Poloniae Pharmaceutica (1985), 42(4), 337-44, database is CAplus.
RCONHNHCOR (R = Me, Et, Ph, 2,4-Cl2C6H3) were converted with NaNH2 in C6H6 into the di-Na salts, which, condensed with Cl(CH2)2S(CH2)3Cl (I) in DMF, yielded 4,5-diacylperhydro-1,4,5-thiadiazocines II. 4,5-Bis(phenylsulfonyl)perhydro-1,4,5-thiadiazocine was prepared analogously from PhSO2NHNHSO2Ph. An analogous reaction with (MeNH)2CO (III) gave thiadiazonine IV (X = CH2), which was also obtained directly from I and III, refluxed in hexanol containing some Na2CO3. The latter method was also used to obtain the dimer IV (X = S) from III and (ClCH2CH2S)2 (V), whereas meso-2,3-diaminobutane-2HCl, condensed under similar conditions with V, yielded VI.
Acta Poloniae Pharmaceutica published new progress about 1002-41-1. 1002-41-1 belongs to chlorides-buliding-blocks, auxiliary class Aliphatic Chain, name is 1,2-Bis(2-chloroethyl)disulfane, and the molecular formula is C8H11NO, Name: 1,2-Bis(2-chloroethyl)disulfane.
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