Wagare, Devendra S. published the artcileHighly efficient microwave-assisted one-pot synthesis of 4-aryl-2-aminothiazoles in aqueous medium, Recommanded Product: 1-(4-Chlorophenyl)thiourea, the publication is Environmental Chemistry Letters (2017), 15(3), 475-479, database is CAplus.
A one-pot protocol for the synthesis of 4-aryl-2-aminothiazoles from the reaction of aromatic ketones, NBS (N-bromosuccinimide) and thioureas under microwave irradiation at 80-85° in PEG (polyethylene glycol)-400 and water as a green reaction medium was developed. The products were obtained in 84-89% yields in 28-32 min. The method had several advantages such as use of green solvent, easy work-up, excellent yield and avoiding use of lachrymatory α-haloketones.
Environmental Chemistry Letters published new progress about 3696-23-9. 3696-23-9 belongs to chlorides-buliding-blocks, auxiliary class Chloride,Thiourea,Amine,Benzene,Amide, name is 1-(4-Chlorophenyl)thiourea, and the molecular formula is C8H7N3, Recommanded Product: 1-(4-Chlorophenyl)thiourea.
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