Development of simple drift tube design for ion mobility spectrometry based on flexible printed circuit board material was written by Chantipmanee, Nattapong;Hauser, Peter C.. And the article was included in Analytica Chimica Acta in 2021.Synthetic Route of C25H46ClN The following contents are mentioned in the article:
A study on the use of flexible printed circuit board material for the construction of drift tubes for ion mobility spectrometry is reported. This is significantly less complicated than the conventional approach based on stacked electrode and insulator rings, as the material can simply be rolled up to obtain a string of circular electrodes. The size and spacing of the electrodes was found to have a strong effect on the resolving power. For an optimized geometry with electrodes of 1.5 mm width at a pitch of 3.5 mm resolving powers of up to 80 were achieved for quaternary amines introduced by electrospray ionization into a drift tube of 10 cm length and an applied voltage of 4200 V. This performance was found to be comparable to that of a conventional drift tube based on stacked rings with otherwise identical geometry and operating conditions. The entire instrument was constructed inhouse. Its utility was demonstrated with the determination of the C12, C14 and C16 benzalkonium ions in several com. cleaning products with limits of detection of 20, 25, and 38μg L-1, resp. This study involved multiple reactions and reactants, such as N-Benzyl-N,N-dimethylhexadecan-1-aminium chloride (cas: 122-18-9Synthetic Route of C25H46ClN).
N-Benzyl-N,N-dimethylhexadecan-1-aminium chloride (cas: 122-18-9) belongs to organic chlorides. Organochlorines stimulate the central nervous system and cause convulsions, tremor, nausea, and mental confusion. Examples are dichlorodiphenyltrichloroethane (DDT), chlordane, lindane, endosulfan, and dieldrin. Alkyl chlorides readily react with amines to give substituted amines. Alkyl chlorides are substituted by softer halides such as the iodide in the Finkelstein reaction.Synthetic Route of C25H46ClN
Referemce:
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics