Safety of 1-Chloro-2-methylbenzene. Nakajima, M; Miyamoto, K; Hirano, K; Uchiyama, M in [Nakajima, Misuzu; Miyamoto, Kazunori; Hirano, Keiichi; Uchiyama, Masanobu] Univ Tokyo, Grad Sch Pharmaceut Sci, Bunkyo Ku, 7-3-1 Hongo, Tokyo 1130033, Japan; [Uchiyama, Masanobu] RIKEN, Adv Elements Chem Lab, CPR, 2-1 Hirosawa, Wako, Saitama 3510198, Japan; [Uchiyama, Masanobu] Shinshu Univ, RISM, Ueda, Nagano 3868567, Japan published Diaryl-lambda(3)-chloranes: Versatile Synthesis and Unique Reactivity as Aryl Cation Equivalent in 2019.0, Cited 53.0. The Name is 1-Chloro-2-methylbenzene. Through research, I have a further understanding and discovery of 95-49-8.
We have developed a versatile, high-yield synthesis of diarylchloroniums/lambda(3)-chloranes through the reaction of various chloroarenes with readily prepared mesityldiazonium tetrakis(pentafluorophenyl)borate under mild conditions. The scope of the reaction is broad, including ArCl, ArBr, and ArI. The diarylchloroniums/lambda(3)-chloranes prepared here show unique reactivity in various respects, enabling intermolecular electrophilic arylation reaction of weak nucleophiles, and chlorane-halogane exchange reaction.
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Reference:
Patent; Nanjing Zhongteng Chemical Co., Ltd.; Zhong Hua; Lu Minshan; Chen Xiuzhen; Liu Qiaobao; Yin Hengbo; Wang Aili; (8 pag.)CN104876790; (2017); B;,
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