Product Details of 87-63-8. Recently I am researching about ARYLATION; PHOTOSWITCHES; DYNAMICS; DYES, Saw an article supported by the ANR JCJC grant ‘2al-Vis-Phot-CH’French National Research Agency (ANR) [ANR-15-CE29-0004-01]. Published in GEORG THIEME VERLAG KG in STUTTGART ,Authors: Jacob, N; Guillemard, L; Wencel-Delord, J. The CAS is 87-63-8. Through research, I have a further understanding and discovery of 2-Chloro-6-methylaniline
Although 3-azoindoles have recently emerged as an appealing family of photoswitch molecules, the synthesis of such compounds has been poorly covered in the literature. Herein a high-yielding and operationally simple protocol is reported allowing the synthesis of 3-azoindoles, featuring important steric hindrance around the azo motif. Remarkably, this C-H coupling is characterized by excellent atom economy and occurs under metal-free conditions, at room temperature, and within few minutes, delivering the expected products in excellent yields (quantitatively in most of the cases). Accordingly, a library of new molecules, with potential applications as photochromic compounds, is prepared.
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Reference:
Patent; ASTRAZENECA AB; NPS PHARMACEUTICALS, INC.; WO2006/20879; (2006); A1;,
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