Electric Literature of 6276-54-6, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 6276-54-6, name is 3-Chloropropan-1-amine hydrochloride, This compound has unique chemical properties. The synthetic route is as follows.
General procedure: 2-Chlorobenzylamine (14.2 g, 0.10 mol), 4-chlorobenzylamine (14.2 g, 0.10 mol), and2,4-dichlorobenzylamine (17.6 g, 0.10 mol) were each dissolved in water (100 cm3),together with phosphorous acid (16.5 g, 0.20 mol), and concentrated hydrochloric acid (d1.18) (100 cm3) was added. The mixture was heated under reflux on a water bath (100C)and formalin (37% aqueous formaldehyde) (0.20 mol) was added portionwise. After 1 hwater was removed by evaporation until crystals appeared. The solution was then cooledand the product was filtered off and recrystallized three times from water to give theproduct as a white crystalline solid, as follows.
The chemical industry reduces the impact on the environment during synthesis 3-Chloropropan-1-amine hydrochloride. I believe this compound will play a more active role in future production and life.
Reference:
Article; Hudson, Harry R.; Koroma, Sia N.; Ojo, Isaac A. O.; Phosphorus, Sulfur and Silicon and the Related Elements; vol. 190; 12; (2015); p. 2187 – 2193;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics